mitsunobu reaction workup

Mono-, di- and tetranuclear rhodium(I) complexes of morpholine and N-methylpiperazine functionalized cyclodiphosph(III)azanes, cis-[( t BuN-μ)2(PNC4H8X)2] (X = O, NMe). Synthesis of Diastereomeric Spirocyclic Nitroxyl Radicals of 3-Imidazoline Series with Two Mesogenic Groups. Alexander N. Prutkov, Mikhail V. Chudinov, Andrey V. Matveev, Lyubov E. Grebenkina, Yulia V. Berezovskaya. Diversity oriented efficient access of trisubstituted purines via sequential regioselective Mitsunobu coupling and SNAr based C6 functionalizations. PPh3O as an Activating Reagent for One-Pot Stereoselective Syntheses of Di- and Polybrominated Esters from Simple Aldehydes. ‘Click chemistry’ in the synthesis of new amphiphilic 1,3-alternate thiacalixarenes. Kohei Yamada, Jie Liu, Munetaka Kunishima. Intermolecular Stereospecific Substitution of Underivatized Enantioenriched Secondary Alcohols by Organocatalysis. ]Methylpalladium Complexes as Intermediates of Stille and Suzuki-Miyaura Cross-Coupling Reactions. Yang Gao, Simin Yang, Yanping Huo, Xiao‐Qiang Hu. Chao Liu, Shan Tang, Liwei Zheng, Dong Liu, Heng Zhang, Aiwen Lei. Nerol Serendipitous alkylation of a Plk1 ligand uncovers a new binding channel. Solvent-free synthesis of δ-carbolines/carbazoles from 3-nitro-2-phenylpyridines/2-nitrobiphenyl derivatives using DPPE as a reducing agent. Bo Teng, Jianfeng Zheng, Huiying Huang, Peiqiang Huang. Shamba Chatterjee, Sandip Guchhait, and Rajib Kumar Goswami . Jia-Dai Zhai, Dongmei Li, Jing Long, Hao-Liang Zhang, Jian-Ping Lin, Chuan-Jiang Qiu, Quan Zhang, and Yue Chen . Reactions are typically done in THF with PPh3 and DEAD (or DIAD) at RT. Chemoenzymatic Synthesis of Racemic and Enantiomerically Pure Phosphaaspartic Acid and Phosphaarginine. Li-Mei Jin, Xue Xu, Hongjian Lu, Xin Cui, Lukasz Wojtas, X. Peter Zhang. Arun K. Ghosh, Cuthbert D. Martyr, Luke A. Kassekert, Prasanth R. Nyalapatla, Melinda Steffey, Johnson Agniswamy, Yuan-Fang Wang, Irene T. Weber, Masayuki Amano, Hiroaki Mitsuya. via The Mitsunobu reaction is an organic reaction that converts an alcohol into a variety of functional groups, such as an ester, using triphenylphosphine and an azodicarboxylate such as diethyl azodicarboxylate (DEAD) or diisopropyl azodicarboxylate(DIAD). Reactions of 5-Fluorouridine with the Terpenols Maki Kurata, Miyabi Hiyama, Takuma Narimatsu, Yuji Hazama, Takashi Ito, Yuhei Hayamizu, Xingping Qiu, Francoise M. Winnik, Hidehumi Akiyama. A Highly Efficient Copper‐Catalyzed C(sp : DNA Building Blocks for a Biomimetic Lipophilization of Nucleic Acids. alternate ‐Aryl Complex. -rich scaffolds for molecular libraries through complexity-generating cascade reactions. Martin Tremblay, Richard C. Bethell, Michael G. Cordingley, Patrick DeRoy, Jianmin Duan, Martin Duplessis, Paul J. Edwards, Anne-Marie Faucher, Ted Halmos, Clint A. James, Cyrille Kuhn, Jean-Éric Lacoste, Louie Lamorte, Steven R. LaPlante, Éric Malenfant, Joannie Minville, Louis Morency, Sébastien Morin, Daniel Rajotte, Patrick Salois, Bruno Simoneau, Sonia Tremblay, Claudio F. Sturino. Daisuke Hirose, Martin Gazvoda, Janez Košmrlj, and Tsuyoshi Taniguchi . A microwave-assisted highly practical chemoselective esterification and amidation of carboxylic acids. Brigitta Bodnár, Erzsébet Mernyák, János Wölfling, Gyula Schneider, Bianka Herman, Mihály Szécsi, Izabella Sinka, István Zupkó, Zoltán Kupihár, Lajos Kovács. Biomimetic Semisynthesis of Arglabin from Parthenolide. Nilesh Jain, Ravi B. Patel, Ashutosh V. Bedekar. Synthesis of tricyclic quinazolinone-iminosugars as potential glycosidase inhibitors via a Mitsunobu reaction. Amol P. Jadhav, Aarti Manchanda, Manish K. Jaiswal, Ravi P. Singh. These metrics are regularly updated to reflect usage leading up to the last few days. Copper-catalyzed oxidative coupling of acids with alkanes involving dehydrogenation: facile access to allylic esters and alkylalkenes. Van Brandt, Juan Antonio Vega, Harrie J.M. Chemoenzymatic preparation of optically active 3-(1H-imidazol-1-yl)cyclohexanol-based ionic liquids: application in organocatalysis and toxicity studies. Thomas Neubauer, Claire Kammerer-Pentier, Thorsten Bach. Joseph Downey, Salvatore Bongarzone, Stefan Hader, Antony D. Gee. Redox-fixable manipulation of planar chirality in late transition metal sandwich compounds; a 1,1′-diphosphacobaltocene/1,1′-diphosphacobaltocenium salt couple. Activating tert-butyl hydroperoxide by chelated vanadates for stereoselectively preparing sidechain-functionalized tetrahydrofurans. Sequential Deoxyfluorination Approach for the Synthesis of Protected α,β,γ-Trifluoro-δ-amino Acids. N6-substituted adenosines. Radiosynthesis of [18F]-Labelled Pro-Nucleotides (ProTides). Recent Advances in Synthesis of Chiral Thioethers. Conception and Realization of Flexible Conjunctive Reagents for Multicomponent Coupling. Synthesis of 7,9-diazabicyclo[4.2.2]decanes as conformationally restricted κ receptor agonists: Fine tuning of the dihedral angle of the ethylenediamine pharmacophore. Daisuke Hirose, Tsuyoshi Taniguchi, Hiroyuki Ishibashi. This article is cited by Alejandro Meco-Navas, Godwin U. Ebiloma, Ana Martín-Domínguez, Irene Martínez-Benayas, Eduardo J. Cueto-Díaz, Amani Saud Alhejely, Emmanuel O. Balogun, Machi Saito, Miho Matsui, Natsumi Arai, Tomoo Shiba, Shigeharu Harada, Harry P. de Koning. Recent Developments in Polymer Analogous Reactions. A concise gram-scale synthesis of ht-13-A via a rhodium-catalyzed intramolecular C–H activation reaction. Terumasa Kato, Shin-ichi Matsuoka, Masato Suzuki. Praneeth Karanam, Ganapuram Madhusudhan Reddy, Srinivasa Rao Koppolu, Wenwei Lin. A Simple and Broadly Applicable C−N Bond Forming Dearomatization Protocol Enabled by Bifunctional Amino Reagents. Qinghe Gao, Shan Liu, Xia Wu, Jingjing Zhang, and Anxin Wu . Matthew D. Helm, Madeleine Da Silva, David Sucunza, Madeleine Helliwell, David J. Procter. Benjamin T. Boyle, Kyle G. Nottingham, Andrew McNally. Henri A. van Kalkeren, Jorick J. Bruins, Floris P. J. T. Rutjes, Floris L. van Delft. Shaaban K. Mohamed, Joel T. Mague, Mehmet Akkurt, Talaat I. El-Emary, Mustafa R. Albayati. Stereoselective photodimerization of alkyl 3-alkoxyl-2-naphthoates. Synthesis of 3′-S-Phosphonomethyl-Modified Nucleoside Phosphonates with a 3′-Deoxy-3′-thio-α-L-threosyl Sugar Moiety. Hubert Hřebabecký, Milan Dejmek, Michal Šála, Helena Mertlíková-Kaiserová, Martin Dračínský, Pieter Leyssen, Johan Neyts, Radim Nencka. Melwin Colaço, Jean Dubois, Johan Wouters. Muhammad Usman, Zhi-Hui Ren, Yao-Yu Wang, Zheng-Hui Guan. Philippe Escavabaja, Jacques Viala, Yoann Coquerel, Jean Rodriguez. Mohammad Navid Soltani Rad, Somayeh Behrouz, Abdo-Reza Nekoei. -pyrazole-3,5-diamines. Shibing Tang, Xingang Xie, Xiaolei Wang, Liuer He, Ke Xu, and Xuegong She . Complex of a 1,10-Phenanthroline-Based Pincer as an Efficient Catalyst for Oxidative Cross Dehydrogenative Coupling of Carboxylic Acids with Unactivated Alkanes. Bastian Tewes, Bastian Frehland, Dirk Schepmann, Dina Robaa, Tanaporn Uengwetwanit, Friedemann Gaube, Thomas Winckler, Wolfgang Sippl, and Bernhard Wünsch . Azodicarboxamides as Template Binding Motifs for the Building of Hydrogen-Bonded Molecular Shuttles. Felicia D’Andrea, Giulia Vagelli, Carlotta Granchi, Lorenzo Guazzelli, Tiziano Tuccinardi, Giulio Poli, Dalila Iacopini, Filippo Minutolo, Valeria Di Bussolo. S. Mahajani, Rowan I. L. Meador, Tomas J. Smith, Sarah E. Canarelli, Arijit A. Adhikari, Jigisha P. Shah, Christopher M. Russo, Daniel R. Wallach, Kyle T. Howard, Alexandra M. Millimaci. Synthesis and pharmacological evaluation of like- and unlike-configured tetrahydro-2-benzazepines with the α-substituted benzyl moiety in the 5-position. Total synthesis and structure–activity relationship study of the potent cAMP signaling agonist (−)-alotaketal A. Abdul Rouf Dar, Mushtaq A. Aga, Brijesh Kumar, Syed Khalid Yousuf, Subhash Chandra Taneja. New para-para Stilbenophanes: Synthesis by McMurry Coupling, Conformational Analysis and Inhibition of Tubulin Polymerisation. Rong Wang, Yijun Zheng, Xiaofu Li, Junxian Chen, Jiaxi Cui, Jie Zhang, Xinhua Wan. A common side reaction is the O-alkylation of the neighboring carbonyl(s). Petra Kollárová-Brázdová, Anna Jirkovská, Galina Karabanovich, Zuzana Pokorná, Hana Bavlovič Piskáčková, Eduard Jirkovský, Jan Kubeš, Olga Lenčová-Popelová, Yvona Mazurová, Michaela Adamcová, Veronika Skalická, Petra Štěrbová-Kovaříková, Jaroslav Roh, Tomáš Šimůnek, Martin Štěrba. -Fluoroaryl Aziridines through Enantioselective Aziridination of Alkenes with Fluoroaryl Azides. Yves Cabon, Duncan Carmichael, Louis Ricard. via redistribute this material, requesters must process their own requests via the RightsLink permission Mariann Szigeti, Zoltán Dobi, and Tibor Soós . Mehdi Adib, Ehsan Sheikhi, Azadeh Deljoush. Sanjay Kumar Varshney, Hiroki Nagayama, Veena Prasad, Hideo Takezoe. Carolina Infante-Rodriguez, Lisianne Domon, Pascal Breuilles, Daniel Uguen. [8.00 g, quant. Nadezhda R. Khasiyatullina, Tamara A. Baronova, Ekaterina V. Mironova, Robert R. Fayzullin, Igor A. Litvinov, Sergey V. Efimov, Rashid Z. Musin, Vladimir V. Klochkov, Vladimir F. Mironov. Kyosuke Kaneda, Risa Naruse, Syota Yamamoto, Teppei Satoh. The material was purified by flash chromatography (solid loading on celite) to provide the product as a white solid. A convenient synthesis of the cytidyl 3′-terminal monomer for solid-phase synthesis of RNG oligonucleotides. Direct Synthesis of Nitriles from Alcohols with Trialkylsilyl Cyanide Using Brønsted Acid Montmorillonite Catalysts.

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